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Beilstein J. Org. Chem. 2018, 14, 1529–1536, doi:10.3762/bjoc.14.129
Graphical Abstract
Scheme 1: Sodium dithionite-mediated reductions under basic conditions.
Figure 1: Uniqsis FlowSyn Stainless Steel Flow reactor.
Figure 2: Flow reactor configuration for the reduction of aldehydes and ketones.
Figure 3: NMR spectra showing the optimisation of the dithionite reduction for the reduction of benzaldehyde.
Figure 4: Selective reduction of an aldehyde in the presence of a ketone.
Figure 5: Flow reactor set-up for the continuous reduction of aldehydes.
Beilstein J. Org. Chem. 2016, 12, 2609–2613, doi:10.3762/bjoc.12.256
Figure 1: Structures of (±)-tashiromine (1) and (±)-epitashiromine (2) showing the systematic numbering of th...
Scheme 1: Reagents and conditions: (i) NH2(CH2)3OH, 250 °C (sealed tube), 18 h, 81%; (ii) Ac2O, pyridine, 0 °...
Scheme 2: Reagents and conditions: (i) Imidazole, PPh3, I2, CH3CN–PhCH3, reflux, 1 h; (ii) p-TsCl, NEt3, DMAP...
Scheme 3: Reagents and conditions: (i) LiAlH4, Et2O, 3 h, 87%.